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Systematic Identification of Organic 6ED
ISBN 0471788740 / 9780471788744 / 0-471-78874-0
Publisher Wiley, John Sons
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Step-by-step instructions on identifying organic compounds. The steps described include elemental analysis, solubility, infrared spectra, nuclear magnetic resonance spectra, mass spectra, classification tests, and preparation of a derivative. Most directions for experiments are described in a micro or mini scale and clean up directions are given at the end of each procedure.
Emphasizes the systematic approach to identifying unknowns.
-- Offers a review of spectroscopy.
-- Discusses infrared, nuclear magnetic resonance, and mass spectroscopy and includes examples of spectra.
-- Discusses chromatography, distillations, and the separation of mixtures. [via]